[Federal Register Volume 70, Number 28 (Friday, February 11, 2005)] [Notices] [Pages 7364-7377] From the Federal Register Online via the Government Publishing Office [www.gpo.gov] [FR Doc No: 05-2714] [[Page 7363]] ----------------------------------------------------------------------- Part IV Environmental Protection Agency ----------------------------------------------------------------------- Fifty-Fifth Report of the TSCA Interagency Testing Committee to the Administrator of the Environmental Protection Agency; Receipt of Report and Request for Comments; Notice Federal Register / Vol. 70, No. 28 / Friday, February 11, 2005 / Notices [[Page 7364]] ----------------------------------------------------------------------- ENVIRONMENTAL PROTECTION AGENCY [OPPT-2004-0130; FRL-7692-1] Fifty-Fifth Report of the TSCA Interagency Testing Committee to the Administrator of the Environmental Protection Agency; Receipt of Report and Request for Comments AGENCY: Environmental Protection Agency (EPA). ACTION: Notice. ----------------------------------------------------------------------- SUMMARY: The Toxic Substances Control Act (TSCA) Interagency Testing Committee (ITC) transmitted its Fifty-Fifth Report to the Administrator of EPA on December 8, 2004. In the 55\th\ ITC Report, which is included with this notice, the ITC is revising the Priority Testing List by adding a category of high production volume (HPV) orphan chemicals and requesting that EPA add these chemicals to the TSCA section 8(a) Preliminary Assessment Information Reporting (PAIR) rule and the TSCA section 8(d) Health and Safety Data Reporting (HaSDR) rule. The ITC is also removing the following chemicals from the Priority Testing List: 3-amino-5-mercapto-1,2,4-triazole; glycoluril; benzenamine, 3-chloro- 2,6-dinitro-N,N-dipropyl-4-(trifluoromethyl)-; stannane, dimethylbis[(1-oxoneodecyl)oxy]-; benzene, 1,3,5-tribromo-2-(2- propenyloxy)-; and1-triazene, 1,3-diphenyl-.]. Since the 55\th\ Report was ITC transmitted to the Administrator and made publicly available on http://www.epa.gov/opptintr/itc/, five HPV orphan chemicals have been removed from the Priority Testing List because chemical manufacturers committed to prepare robust summaries for these chemicals in response to the HPV Challenge Program. The ITC encourages other manufacturers to make similar commitments so their chemicals can be removed from the Priority Testing List and potentially avoid being added to PAIR and HaSDR rules. DATES: Comments, identified by docket identification (ID) number OPPT- 2004-0130, must be received on or before March 14, 2005. ADDRESSES: Comments may be submitted electronically, by mail, or through hand delivery/courier. Follow the detailed instructions as provided in Unit I. of the SUPPLEMENTARY INFORMATION. FOR FURTHER INFORMATION CONTACT: For general information contact: Colby Lintner, Regulatory Coordinator, Environmental Assistance Division (7408M), Office of Pollution Prevention and Toxics, Environmental Protection Agency, 1200 Pennsylvania Ave., NW., Washington, DC 20460-0001; telephone number: (202) 554-1404; e-mail address: TSCA-Hotline@epa.gov. For technical information contact: John D. Walker, Director, TSCA Interagency Testing Committee (7401), Office of Pollution Prevention and Toxics, Environmental Protection Agency, 1200 Pennsylvania Ave., NW., Washington, DC 20460-0001; e-mail address: walker.johnd@epa.gov. SUPPLEMENTARY INFORMATION: I. General Information A. Does this Action Apply to Me? This notice is directed to the public in general. It may, however, be of particular interest to you if you manufacture (defined by statute to include import) and/or process TSCA-covered chemicals and you may be identified by the North American Industrial Classification System (NAICS) codes 325 and 32411. Because this notice is directed to the general public and other entities may also be interested, the Agency has not attempted to describe all the specific entities that may be interested in this action. If you have any questions regarding the applicability of this action to a particular entity, consult the technical person listed under FOR FURTHER INFORMATION CONTACT. B. How Can I Get Copies of this Document and Other Related Information? 1. Docket. EPA has established an official public docket for this action under docket ID number OPPT-2004-0130. The official public docket consists of the documents specifically referenced in this action, any public comments received, and other information related to this action. Although a part of the official docket, the public docket does not include Confidential Business Information (CBI) or other information whose disclosure is restricted by statute. The official public docket is the collection of materials that is available for public viewing at the EPA Docket Center, Rm. B102-Reading Room, EPA West, 1301 Constitution Ave., NW., Washington, DC. The EPA Docket Center is open from 8:30 a.m. to 4:30 p.m., Monday through Friday, excluding legal holidays. The EPA Docket Center Reading Room telephone number is (202) 566-1744 and the telephone number for the OPPT Docket, which is located in EPA Docket Center, is (202) 566-0280. 2. Electronic access. You may access this Federal Register document electronically through the EPA Internet under the ``Federal Register'' listings at http://www.epa.gov/fedrgstr/. You may also access additional information about the ITC at http://www.epa.gov/opptintr/ itc/ or through the web site for the Office of Prevention, Pesticides and Toxic Substances (OPPTS) at http://www.epa.gov/opptsfrs/home/ opptsim.htm/. An electronic version of the public docket is available through EPA's electronic public docket and comment system, EPA Dockets. You may use EPA Dockets at http://www.epa.gov/edocket/ to submit or view public comments, access the index listing of the contents of the official public docket, and to access those documents in the public docket that are available electronically. Although not all docket materials may be available electronically, you may still access any of the publicly available docket materials through the docket facility identified in Unit I.B.1. Once in the system, select ``search,'' then key in the appropriate docket ID number. Certain types of information will not be placed in the EPA Dockets. Information claimed as CBI and other information whose disclosure is restricted by statute, which is not included in the official public docket, will not be available for public viewing in EPA's electronic public docket. EPA's policy is that copyrighted material will not be placed in EPA's electronic public docket but will be available only in printed, paper form in the official public docket. To the extent feasible, publicly available docket materials will be made available in EPA's electronic public docket. When a document is selected from the index list in EPA Dockets, the system will identify whether the document is available for viewing in EPA's electronic public docket. Although not all docket materials may be available electronically, you may still access any of the publicly available docket materials through the docket facility identified in Unit I.B.1. EPA intends to work towards providing electronic access to all of the publicly available docket materials through EPA's electronic public docket. For public commenters, it is important to note that EPA's policy is that public comments, whether submitted electronically or in paper, will be made available for public viewing in EPA's electronic public docket as EPA receives them and without change, unless the comment contains copyrighted material, CBI, or other information whose disclosure is restricted by statute. When EPA identifies a comment containing copyrighted material, EPA will provide [[Page 7365]] a reference to that material in the version of the comment that is placed in EPA's electronic public docket. The entire printed comment, including the copyrighted material, will be available in the public docket. Public comments submitted on computer disks that are mailed or delivered to the docket will be transferred to EPA's electronic public docket. Public comments that are mailed or delivered to the docket will be scanned and placed in EPA's electronic public docket. Where practical, physical objects will be photographed, and the photograph will be placed in EPA's electronic public docket along with a brief description written by the docket staff. C. How and to Whom Do I Submit Comments? You may submit comments electronically, by mail, or through hand delivery/courier. To ensure proper receipt by EPA, identify the appropriate docket ID number in the subject line on the first page of your comment. Please ensure that your comments are submitted within the specified comment period. Comments received after the close of the comment period will be marked ``late.'' EPA is not required to consider these late comments. If you wish to submit CBI or information that is otherwise protected by statute, please follow the instructions in Unit I.D. Do not use EPA Dockets or e-mail to submit CBI or information protected by statute. 1. Electronically. If you submit an electronic comment as prescribed in this unit, EPA recommends that you include your name, mailing address, and an e-mail address or other contact information in the body of your comment. Also include this contact information on the outside of any disk or CD ROM you submit, and in any cover letter accompanying the disk or CD ROM. This ensures that you can be identified as the submitter of the comment and allows EPA to contact you in case EPA cannot read your comment due to technical difficulties or needs further information on the substance of your comment. EPA's policy is that EPA will not edit your comment, and any identifying or contact information provided in the body of a comment will be included as part of the comment that is placed in the official public docket, and made available in EPA's electronic public docket. If EPA cannot read your comment due to technical difficulties and cannot contact you for clarification, EPA may not be able to consider your comment. i. EPA Dockets. Your use of EPA's electronic public docket to submit comments to EPA electronically is EPA's preferred method for receiving comments. Go directly to EPA Dockets at http://www.epa.gov/ edocket/, and follow the online instructions for submitting comments. Once in the system, select ``search,'' and then key in docket ID number OPPT-2004-0130. The system is an `` anonymous access'' system, which means EPA will not know your identity, e-mail address, or other contact information unless you provide it in the body of your comment. ii. E-mail. Comments may be sent by e-mail to oppt.ncic@epa.gov, Attention: Docket ID Number OPPT-2004-0130. In contrast to EPA's electronic public docket, EPA's e-mail system is not an ``anonymous access'' system. If you send an e-mail comment directly to the docket without going through EPA's electronic public docket, EPA's e-mail system automatically captures your e-mail address. E-mail addresses that are automatically captured by EPA's e-mail system are included as part of the comment that is placed in the official public docket, and made available in EPA's electronic public docket. iii. Disk or CD ROM. You may submit comments on a disk or CD ROM that you mail to the mailing address identified in Unit I.C.2. These electronic submissions will be accepted in WordPerfect or ASCII file format. Avoid the use of special characters and any form of encryption. 2. By mail. Send your comments to: Document Control Office (7407M), Office of Pollution Prevention and Toxics (OPPT), Environmental Protection Agency, 1200 Pennsylvania Ave., NW., Washington, DC 20460- 0001. 3. By hand delivery or courier. Deliver your comments to: OPPT Document Control Office (DCO), EPA East Bldg., Rm. 6428, 1201 Constitution Ave., NW., Washington, DC. Attention: Docket ID Number OPPT-2004-0130. The DCO is open from 8 a.m. to 4 p.m., Monday through Friday, excluding legal holidays. The telephone number for the DCO is (202) 564-8930. D. How Should I Submit CBI to the Agency? Do not submit information that you consider to be CBI electronically through EPA's electronic public docket or by e-mail. You may claim information that you submit to EPA as CBI by marking any part or all of that information as CBI (if you submit CBI on disk or CD ROM, mark the outside of the disk or CD ROM as CBI and then identify electronically within the disk or CD ROM the specific information that is CBI). Information so marked will not be disclosed except in accordance with procedures set forth in 40 CFR part 2. In addition to one complete version of the comment that includes any information claimed as CBI, a copy of the comment that does not contain the information claimed as CBI must be submitted for inclusion in the public docket and EPA's electronic public docket. If you submit the copy that does not contain CBI on disk or CD ROM, mark the outside of the disk or CD ROM clearly that it does not contain CBI. Information not marked as CBI will be included in the public docket and EPA's electronic public docket without prior notice. If you have any questions about CBI or the procedures for claiming CBI, please consult the technical person listed under FOR FURTHER INFORMATION CONTACT. E. What Should I Consider as I Prepare My Comments for EPA? We invite you to provide your views and comments on the ITC's 55\th\ Report. You may find the following suggestions helpful for preparing your comments: 1. Explain your views as clearly as possible. 2. Describe any assumptions that you used. 3. Provide copies of any technical information and/or data you used that support your views. 4. Provide specific examples to illustrate your concerns. 5. Make sure to submit your comments by the deadline in this notice. 6. To ensure proper receipt by EPA, be sure to identify the docket ID number assigned to this action in the subject line on the first page of your response. You may also provide the name, date, and Federal Register citation. II. Background The Toxic Substances Control Act (TSCA) (15 U.S.C. 260l et seq.) authorizes the Administrator of the EPA to promulgate regulations under section 4(a) of TSCA requiring testing of chemicals and chemical groups in order to develop data relevant to determining the risks that such chemicals and chemical groups may present to health or the environment. Section 4(e) of TSCA established the ITC to recommend chemicals and chemical groups to the Administrator of the EPA for priority testing consideration. Section 4(e) of TSCA directs the ITC to revise the TSCA section 4(e) Priority Testing List at least every 6 months. A. The ITC's 55\th\ Report The 55\th\ ITC Report was transmitted to EPA's Administrator on December 8, [[Page 7366]] 2004, and is included in this notice. In the 55\th\ ITC Report, the ITC is revising the Priority Testing List by adding a category of HPV orphan chemicals and requesting that EPA add these chemicals to the TSCA section 8(a) PAIR rule and the TSCA section 8(d) HaSDR rule. The ITC is also removing the following chemicals from the Priority Testing List: 3-amino-5-mercapto-1,2,4-triazole; glycoluril; benzenamine, 3- chloro-2,6-dinitro-N,N-dipropyl-4-(trifluoromethyl)-; stannane, dimethylbis[(1-oxoneodecyl)oxy]-; benzene, 1,3,5-tribromo-2-(2- propenyloxy)-; and 1-triazene, 1,3-diphenyl-. B. Status of the Priority Testing List The current TSCA 4(e) Priority Testing List as of December 2004 can be found in Table 1 of the 55\th\ ITC Report, which is included in this notice. List of Subjects Environmental protection, Chemicals, Hazardous substances. Dated: February 3, 2005. Charles M. Auer, Director, Office of Pollution Prevention and Toxics. Fifty-Fifth Report of the TSCA Interagency Testing Committee to the Administrator, U.S. Environmental Protection Agency Table of Contents Summary I. Background II. TSCA Section 8 Reporting A. TSCA Ssection 8 Reporting Rules B. ITC's Use of TSCA Section 8 and Other Information C. Previous Requests to Add Chemicals to the TSCA Section 8(a) PAIR Rule D. New Requests to Add Chemicals to the TSCA Section 8(a) PAIR and 8(d) HaSDR Rules III. ITC's Activities During this Reporting Period (May to November 2004) IV. Revisions to the TSCA Section 4(e) Priority Testing List A. Chemicals Added to the Priority Testing List: HPV Orphan Chemicals B. Chemicals Removed From the Priority Testing List 1. 3-Amino-5-mercapto-1,2,4-triazole. 2. Glycoluril. 3. Benzenamine, 3-chloro-2,6-dinitro-N,N-dipropyl-4- (trifluoromethyl)-. 4. Stannane, dimethylbis[(1-oxoneodecyl)oxy]-. 5. Benzene, 1,3,5-tribromo-2-(2-propenyloxy)-. 6. 1-Triazene, 1,3-diphenyl-. V. References VI. The TSCA Interagency Testing Committee Summary In this 55\th\ ITC Report, the ITC is revising the Priority Testing List by adding a category of High Production Volume (HPV) orphan chemicals and requesting that EPA add these chemicals to the Toxic Substances Control Act (TSCA) section 8(a) Preliminary Assessment Information Reporting (PAIR) rule and the TSCA section 8(d) Health and Safety Data Reporting (HaSDR) rule. The ITC is also removing the following chemicals from the Priority Testing List: 3- amino-5-mercapto-1,2,4-triazole; glycoluril; benzenamine, 3-chloro- 2,6-dinitro-N,N-dipropyl-4-(trifluoromethyl)-; stannane, dimethylbis[(1-oxoneodecyl)oxy]-; benzene, 1,3,5-tribromo-2-(2- propenyloxy)-; and 1-triazene, 1,3-diphenyl-. The TSCA section 4(e) Priority Testing List is Table 1 of this unit. Table 1.--The TSCA Section 4(e) Priority Testing List (November 2004) ---------------------------------------------------------------------------------------------------------------- ITC Report Date Chemical name/group Action ---------------------------------------------------------------------------------------------------------------- 31 January 1993 13 Chemicals with Designated insufficient dermal absorption rate data --------------------------------------------------------------- --------------------------------------------------------------- --------------------------------------------------------------- --------------------------------------------------------------- --------------------------------------------------------------- --------------------------------------------------------------- --------------------------------------------------------------- --------------------------------------------------------------- --------------------------------------------------------------- ---------------------------------------------------------------------------------------------------------------- I. Background The ITC was established by section 4(e) of TSCA ``to make recommendations to the Administrator respecting the chemical substances and mixtures to which the Administrator should give priority consideration for the promulgation of rules for testing under section 4(a).... At least every six months ..., the Committee shall make such revisions to the Priority Testing List as it determines to be necessary and transmit them to the Administrator together with the Committee's reasons for the revisions'' (Public Law 94-469, 90 Stat. 2003 et seq., 15 U.S.C. 2601 et seq.). ITC Reports are available from the ITC's web site (http://www.epa.gov/ opptintr/itc/) within a few days of submission to the Administrator and from the EPA's web site http://www.epa.gov/fedrgstr/ after publication in the Federal Register. The ITC produces its revisions to the Priority Testing List with administrative and technical support from the ITC Staff and ITC Members and their U.S. Government organizations, and contract support provided by EPA. ITC Members and Staff are listed at the end of this report. II. TSCA Section 8 Reporting A. TSCA Section 8 Reporting Rules Following receipt of the ITC's Report (and the revised Priority Testing List) by the EPA Administrator, the EPA's Office of Pollution Prevention and Toxics (OPPT) may add the chemicals from the revised Priority Testing List to the TSCA section 8(a) Preliminary Assessment Information Reporting (PAIR) and TSCA section 8(d) Health and Safety Data Reporting (HaSDR) rules. The PAIR rule requires producers and importers of chemicals added to the Priority Testing List to submit production and exposure reports (http:// www.epa.gov/opptintr/chemtest/pairform.pdf/). The HaSDR rule requires producers, importers and processors of all chemicals added to the Priority Testing List to submit unpublished health and safety studies under TSCA section 8(d) that must be in compliance with the revised HaSDR rule (Ref. 1). All submissions must be received by the EPA within 90 days of the reporting rules Federal Register publication date. [[Page 7367]] B. ITC's Use of TSCA Section 8 and Other Information The ITC's use of TSCA section 8 and other information is described in previous ITC Reports (http://www.epa.gov/opptintr/itc/ rptmain.htm/). C. Previous Requests to Add Chemicals to the TSCA Section 8(a) PAIR Rule In its 53\rd\ Report, the ITC requested that EPA add 3 pyridinamines and 20 tungsten compounds to the TSCA section 8(a) PAIR rule (Ref. 2). On December 7, 2004, EPA issued a final rule, pursuant to TSCA section 8(a) requiring producers and importers of these 23 chemicals to report production, importation, and exposure data to EPA (Ref. 3). D. New Requests to Add Chemicals to the TSCA Section 8(a) PAIR and 8(d) HaSDR Rules In this report, the ITC is requesting that EPA add the HPV orphan chemicals listed in Appendix A to the TSCA section 8(a) PAIR and 8(d) HaSDR rules. The ITC is requesting that these HPV orphan chemicals be added to the TSCA section 8(a) PAIR and 8(d) HaSDR rules because no voluntary studies have been submitted to the EPA in response to the HPV Challenge Program (http://www.epa.gov/opptintr/ chemrtk/volchall.htm/). III. ITC's Activities During this Reporting Period (May to November 2004) During this reporting period, the ITC reviewed the reports submitted in response to the June 11, 2003, PAIR rule (Ref. 4) and the May 4, 2004, TSCA section 8(d) HaSDR rule (Ref. 5). The ITC is continuing to review these reports. The ITC also met with EPA to discuss procedures for making data publicly available on HPV orphan chemicals (HPV chemicals for which no sponsors have volunteered to develop and submit robust summaries to the EPA). The ITC's discussions with EPA are described in section IV. of this report. As noted in the 51\st\ and 54\th\ ITC Reports (Refs. 6 and 7), the ITC continues to request the following information on vanadium compounds: 1. Recent non-CBI estimates of annual production or importation volume data and trends, and use information, including percentages of production or importation that are associated with different uses. 2. Estimates of the number of humans and concentrations of vanadium chemicals to which humans may be exposed in each relevant manufacturing or processing scenario. 3. Health effects data including pharmacokinetics, genotoxicity, subchronic toxicity, reproductive and developmental toxicity, and any human data from occupationally exposed workers. The ITC seeks this information in order to adequately assess the extent and degree of exposure and potential hazard associated with the various forms of vanadium. In addition, the ITC is concerned that some of these compounds may be released into fly ash ponds at power plants, petroleum and chemical refineries, and mining sites and could be toxic to avian and wildlife species as exemplified by a recent report of dead and dying Canada geese at a petroleum refinery fly ash pond in Delaware. In these geese, the vanadium concentrations in pooled liver and kidney samples were 57 and 226 [mu]g/gram (g) dry weight, respectively. Background concentrations of vanadium in various tissues of higher vertebrates, including waterfowl, rarely exceed 1 [mu]g/g dry weight. Limited data are available on vanadium toxicity in birds and other wildlife making it difficult to interpret the findings from the geese die-off. The ITC knows that vanadium is released into impoundments at 172 facilities in 33 states and that the TRI does not have vanadium concentrations for these impoundments. The ITC is soliciting data on concentrations and species of vanadium compounds in impoundments at power plants, petroleum and chemical refineries, and mining sites and information on the use, release, and presence of vanadium compounds at these facilities. The ITC needs these data and information to determine if avian wildlife in the vicinity of the 172 facilities are at risk from exposure to vanadium compounds. If you have any questions regarding the applicability of this action to a particular entity, consult the technical person listed under FOR FURTHER INFORMATION CONTACT. IV. Revisions to the TSCA Section 4(e) Priority Testing List A. Chemicals Added to the Priority Testing List: HPV Orphan Chemicals 1. Recommendation. EPA requests that the ITC add the category HPV orphan chemicals listed in Appendix A of this report to the Priority Testing List to obtain importation, production, use, and exposure information as well as unpublished physical/chemical property, environmental fate, health effects, and ecological effects information to meet U.S. Government data needs. 2. Rationale for recommendation. While the success of the HPV Challenge Program has been significant, hundreds of chemicals that were eligible for sponsorship in the Program continue to remain unsponsored. These chemicals are referred to as ``orphans.'' There is little or no publicly available information regarding the potential hazards associated with these chemicals. EPA remains committed to obtain basic screening level hazard information on these chemicals through voluntary sponsorship, as well as through TSCA information gathering and test rules, as necessary. 3. Supporting information. In developing the list of HPV orphan chemicals presented in Appendix A of this report, EPA considered all of the HPV orphan chemicals and then removed selected HPV orphan chemicals. The HPV orphan chemicals presented in Appendix A of this report do not include those HPV orphan chemicals that: a. Had 2002 Inventory Update rule reported production/ importation volumes > one million pounds (http://www.epa.gov/oppt/ iur/iur02/index.htm/ ) and were proposed for testing in the first HPV test rule (Ref. 8). b. Meet the ``No Longer HPV'' criteria (i.e., chemicals with production/importation volumes < 1 million pounds based on 1998 and 2002 Inventory Update Rule data (http://www.epa.gov/oppt/iur/iur02/ index.htm/)). c. Are being considered for a second HPV TSCA section 4 test rule because they may meet the TSCA section 4(a)(1)(B) statutory requirements. At EPA's request, the ITC encourages manufacturers of these chemicals to visit the EPA's HPV Challenge Program web site (http:// www.epa.gov/opptintr/chemrtk/volchall.htm/) and to make a commitment to sponsor these chemicals at the present time, before regulatory actions are initiated. EPA will initiate development of TSCA section 8(a) PAIR and 8(d) HaSDR rules soon after these chemicals are added to the Priority Testing List and the ITC's 55\th\ Report is published in the Federal Register. Also at EPA's request, the ITC encourages the submission of robust summaries of studies submitted under the TSCA section 8(d) HaSDR rule to facilitate EPA's review of the unpublished TSCA section 8(d) studies (see USEPA. 1999. Draft Guidance on Developing Robust Summaries. October 22, 1999 (http:// www.epa.gov/chemrtk/robsumgd.htm/)). While some of the HPV orphan chemicals have been previously added to the TSCA section 8(d) HaSDR rule, all of the sunset dates for these chemicals have expired (see Appendix A of this report), thus new and so far unreported studies would need to be submitted. Information about the environmental fate and potential hazards associated with these chemicals when combined with information about exposure and uses will allow the EPA and others to evaluate and prioritize potential health and environmental effects and determine the need for test rules under TSCA section 4(a). If you have any questions regarding the applicability of this action to a particular entity, consult the technical person listed under FOR FURTHER INFORMATION CONTACT. 4. Information needs. For each individual substance listed in Appendix A of this report, EPA needs the following information to assess the extent and degree of exposure and potential hazard associated with these substances: a. Production, importation, processing, use and associated exposure information that is captured under the TSCA section 8(a) PAIR form. b. Unpublished studies of: i. Physical/chemical properties and environmental fate for the properties listed in 40 CFR 716.50 as well as melting point and boiling point. ii. Health effects including pharmacokinetics, genotoxicity, acute toxicity, subacute toxicity, subchronic toxicity, chronic toxicity, reproductive toxicity, developmental toxicity, immunotoxicity, neurotoxicity, and oncogenicity/carcinogenicity. iii. Ecological effects including acute and chronic toxicity studies of aquatic and terrestrial vertebrates and invertebrates and aquatic plants. c. Only studies where the recommended HPV orphan chemical is >= 90% of the test substance by weight should be submitted. In [[Page 7368]] addition, only studies that were conducted using TSCA, Federal Insecticide, Fungicide, and Rodenticide Act (FIFRA), Organization for Economic Cooperation and Development (OECD), or other internationally accepted test guidelines or voluntary consensus standards should be submitted. Studies performed where the recommended HPV orphan chemical is < 90% of the test substance by weight are not requested at this time. B. Chemicals Removed From the Priority Testing List 1. 3-Amino-5-mercapto-1,2,4-triazole. 3-Amino-5-mercapto-1,2,4- triazole (Chemical Abstracts Service Registry Number (CAS No.) 16691-43-3 ) was added to the Priority Testing List in the ITC's 42\nd\ Report to obtain annual production/importation volumes and trends, use, exposure, and health effects data (Ref. 9). The addition was based on concerns that 3-amino-5-mercapto-1,2,4- triazole was structurally related to 3-amino-1,2,4-triazole (Amitrol[reg]), a herbicide that affects thyroid hormone activity (Ref. 10). In response to the ITC's request, the EPA added 3-amino- 5-mercapto-1,2,4-triazole to the July 24, 2000, PAIR rule (Ref. 11) and the May 4, 2004 HaSDR rule (Ref. 5). Numerous studies were submitted in response to the HaSDR rule. These studies are summarized in this unit. 3-Amino-5-mercapto-1,2,4-triazole was positive in the mouse bone marrow micronucleus test, clastogenic to rat lymphocytes, but not mutagenic in the Ames assay using strains TA98, 100, 1535, and 1537 or in the E. coli assay, using strain WP2 uvrA-. 3-Amino-5-mercapto-1,2,4-triazole was a mild eye and skin irritant, but not a skin sensitizer. In a 4-week inhalation study the no observed effect level of 3-amino-5-mercapto-1,2,4-triazole was 20 milligram/meter cubed (mg/m\3\). 3-Amino-5-mercapto-1,2,4-triazole is being removed from the Priority Testing List because information submitted in response to the PAIR rule suggested that 3-amino-5-mercapto-1,2,4-triazole is an on-site intermediate and the production/importation volumes were lower than the 250,000 pounds of 3-amino-5-mercapto-1,2,4-triazole imported into the United States in 1993 (Ref. 9). 2. Glycoluril. Glycoluril (CAS No. 496-46-8) was also added to the Priority Testing List in the ITC's 42\nd\ Report to obtain annual production/importation volumes and trends, use, exposure, and health effects data. The addition was based on a potential for human exposure and a suspicion of carcinogenicity (Ref. 9). In response to the ITC's request, the EPA added glycoluril to the July 24, 2000 PAIR rule (Ref. 11) and the May 4, 2004 HaSDR rule (Ref. 5). No studies were submitted in response to the HaSDR rule. Glycoluril is being removed from the Priority Testing List because information submitted in response to the PAIR rule suggested that glycoluril is an on-site intermediate and the production/ importation volumes were less than the 10,000 to 1,000,000 pounds of non-CBI annual production/importation volumes reported to the EPA in 1986, 1990, and 1994 (Ref. 9). 3. Benzenamine, 3-chloro-2,6-dinitro-N,N-dipropyl-4- (trifluoromethyl)-. Benzenamine, 3-chloro-2,6-dinitro-N,N-dipropyl- 4-(trifluoromethyl)- (aka 3-Chlorotrifluralin (CAS No. 29091-20-1) was added to the Priority Testing List in the ITC's 48\th\ Report to obtain information on uses, exposures, environmental releases, pharmacokinetics, subchronic toxicity, mutagenicity, reproductive and developmental effects, carcinogenicity, and ecological effects (Ref. 12). Benzenamine, 3-chloro-2,6-dinitro-N,N-dipropyl-4- (trifluoromethyl)- was added to the Priority Testing List because it has an estimated bioconcentration factor (BCF) of 7,700 and is a chlorinated analog of trifluralin (CAS No. 1582-09-8), the herbicide that causes adverse effects in experimental animals and is considered to be a possible human carcinogen by the EPA (Ref. 12). In response to the ITC's request, the EPA added benzenamine, 3- chloro-2,6-dinitro-N,N-dipropyl-4-(trifluoromethyl)- to the June 11, 2003 PAIR rule (Ref. 4) and the May 4, 2004 TSCA section 8(d) HaSDR rule (Ref. 5). No information was submitted in response to the PAIR or HaSDR rules. The ITC is removing benzenamine, 3-chloro-2,6- dinitro-N,N-dipropyl-4-(trifluoromethyl)- from the Priority Testing List because the PAIR rule did not provide any additional exposure information implying that benzenamine, 3-chloro-2,6-dinitro-N,N- dipropyl-4-(trifluoromethyl)- is not produced at greater than 1,000 pounds per site. 4. Stannane, dimethylbis[(1-oxoneodecyl)oxy]-. Stannane, dimethylbis[(1-oxoneodecyl)oxy]- (CAS No. 68928-76-7) was added to the Priority Testing List in the ITC's 49\th\ Report to obtain use, exposure, environmental fate, health effects, and ecological effects data (Ref. 13). Stannane, dimethylbis[(1-oxoneodecyl)oxy]- was added to the Priority Testing List because it has an estimated BCF of 8,600 and signs of toxicity, including neurotoxic effects that were observed in a rat oral gavage study (Ref. 13). In response to the ITC's request, the EPA added stannane, dimethylbis[(1-oxoneodecyl)oxy]- to the June 11, 2003 PAIR rule (Ref. 4) and the May 4, 2004 TSCA section 8(d) HaSDR rule (Ref. 5). No information was submitted in response to the HaSDR rule. The ITC is removing stannane, dimethylbis[(1-oxoneodecyl)oxy]- from the Priority Testing List because the information submitted in response to the PAIR rule suggested that the production/importation volumes of stannane, dimethylbis[(1-oxoneodecyl)oxy]- were not greater than the 10,000-500,000 pounds of non-CBI production/importation volumes reported to the EPA in 2002 (http://www.epa.gov/oppt/iur/iur02/ index.htm/). 5. Benzene, 1,3,5-tribromo-2-(2-propenyloxy)-. Benzene, 1,3,5- tribromo-2-(2-propenyloxy)- (CAS No. 3278-89-5) was added to the Priority Testing List in the ITC's 50\th\ Report to obtain use, exposure, environmental fate, health effects, and ecological effects data (Ref. 14). Benzene, 1,3,5-tribromo-2-(2-propenyloxy)- was added to the Priority Testing List because of an estimated BCF of 4,000 and potential for exposure from its use as a flame retardant for expanded polystyrene insulation board (Ref. 14). In response to the ITC's request, the EPA added benzene, 1,3,5- tribromo-2-(2-propenyloxy)- to the June 11, 2003 PAIR rule (Ref. 4) and the May 4, 2004 TSCA section 8(d) HaSDR rule (Ref. 5). Information submitted in response to the HaSDR rule indicated that the concentrated chemical may be slightly irritating to the skin. The ITC is removing benzene, 1,3,5-tribromo-2-(2-propenyloxy)- from the Priority Testing List because the information submitted in response to the PAIR rule suggested that the production/importation volumes of benzene, 1,3,5-tribromo-2-(2-propenyloxy)- were not greater than 10,000-500,000 pounds of non-CBI production/importation volumes reported to the EPA in 2002 (http://www.epa.gov/oppt/iur/ iur02/index.htm/). 6. 1-Triazene, 1,3-diphenyl-. 1-Triazene, 1,3-diphenyl- (aka diazoaminobenzene (CAS No. 136-35-6) was added to the Priority Testing List in the ITC's 50\th\ Report to obtain annual production/ importation volumes and trends, use, exposure, and health effects data (Ref. 14). 1-Triazene, 1,3-diphenyl- was added to the Priority Testing List because it is a predicted carcinogen based on its metabolism and similarity in toxic effects to benzene and aniline (Ref. 14). In response to the ITC's request, the EPA added 1-triazene, 1,3- diphenyl- to the June 11, 2003 PAIR rule (Ref. 4) and the May 4, 2004 TSCA section 8(d) HaSDR rule (Ref. 5). No information was submitted in response to the PAIR or HaSDR rules. The ITC is removing 1-triazene, 1,3-diphenyl- from the Priority Testing List because the PAIR rule did not provide any additional exposure information implying that 1-triazene, 1,3-diphenyl- is not produced at greater than 1,000 pounds per site. V. References 1. EPA. 1998. Revisions to Reporting Regulations Under TSCA Section 8(d). Direct Final Rule. Federal Register (63 FR 15765, April 1, 1998) (FRL-5750-4). Available online at: http:// www.epa.gov/fedrgstr/. 2. ITC. 2004. Fifty-Third Report of the ITC. Federal Register (69 FR 2467, January 15, 2004) (FRL-7335-2). Available online at: http://www.epa.gov/fedrgstr/. 3. EPA. 2004. Preliminary Assessment Information Reporting; Addition of Certain Chemicals. Final Rule. Federal Register (69 FR 70552, December 7, 2004) (FRL-7366-8). Available online at: http:// www.epa.gov/fedrgstr/. 4. EPA. 2003. Preliminary Assessment Information Reporting; Addition of Certain Chemicals. Final Rule. Federal Register (68 FR 34832, June 11, 2003) (FRL-7306-7). Available online at: http:// www.epa.gov/fedrgstr/. 5. EPA. 2004. Health and Safety Data Reporting; Addition of Certain Chemicals. Final Rule. Federal Register (69 FR 24517, May 4, 2004) (FRL-7322-8). Available online at: http://www.epa.gov/ fedrgstr/. 6. ITC. 2003. Fifty-First Report of the ITC. Federal Register (68 FR 8976, February 26, 2003) (FRL-7285-7). Available online at: http://www.epa.gov/fedrgstr/. 7. ITC. 2004. Fifty-Fourth Report of the ITC. Federal Register (69 FR 33527, June 15, 2004) (FRL-7359-6). Available online at: http://www.epa.gov/fedrgstr/. 8. EPA. 2000. Testing of Certain High Production Volume Chemicals. Proposed [[Page 7369]] Rule. Federal Register (65 FR 81658, December 26, 2000) (FRL-6758- 4). Available online at: http://www.epa.gov/fedrgstr/. 9. ITC. 1998. Forty-Second Report of the ITC. Federal Register (63 FR 42554, August 7, 1998) (FRL-5797-8). Available online at: http://www.epa.gov/fedrgstr/. 10. Takaoka, M., M. Teranishi, and S. Manabe. 1994. Structure- Activity Relationships in 5-Substituted 3-Amino-1,2,4-Triazoles- Induced Goiters in Rats. Journal of Toxicology and Pathology. 7:429- 434. 11. EPA. 2000. Preliminary Assessment Information Reporting; Addition of Certain Chemicals. Final Rule. Federal Register (65 FR 45535, July 24, 2000) (FRL-6597-3). Available online at: http:// www.epa.gov/fedrgstr/. 12. ITC. 2001. Forty-Eighth Report of the ITC. Federal Register (66 FR 51276, October 5, 2001) (FRL-6786-7). Available online at: http://www.epa.gov/fedrgstr/. 13. ITC. 2002. Forty-Ninth Report of the ITC. Federal Register (67 FR 10298, March 6, 2002) (FRL-6820-8). Available online at: http://www.epa.gov/fedrgstr/. 14. ITC. 2002. Fiftieth Report of the ITC. Federal Register (67 FR 49530, July 30, 2002) (FRL-7183-7). Available online at: http:// www.epa.gov/fedrgstr/. VI. The TSCA Interagency Testing Committee Statutory Organizations and Their Representatives Council on Environmental Quality Vacant Department of Commerce National Institute of Standards and Technology Dianne Poster, Member Peter Barker, Alternate National Oceanographic and AtmosphericAdministration Thomas P. O'Connor, Member, Chair Teri Rowles, Alternate Environmental Protection Agency Gerry Brown, Member Paul Campanella, Alternate National Cancer Institute Alan Poland, Member Shen Yang, Alternate National Institute of Environmental Health Sciences Barbara Shane, Member Scott Masten, Alternate National Institute for Occupational Safety and Health Mark Toraason, Member Dennis W. Lynch, Alternate National Science Foundation Marge Cavanaugh, Member Parag R. Chitnis, Alternate Occupational Safety and Health Administration Maureen Ruskin, Member Liaison Organizations and Their Representatives Agency for Toxic Substances and Disease Registry Daphne Moffett, Member Consumer Product Safety Commission Treye Thomas, Member Jacqueline Ferrante, Alternate Department of Agriculture Clifford P. Rice, Member, Vice Chair Laura L. McConnell, Alternate Department of Defense Warren Jederberg, Member Department of the Interior Barnett A. Rattner, Member Food and Drug Administration Kirk Arvidson, Alternate Ronald F. Chanderbhan, Alternate National Library of Medicine Vera W. Hudson, Member National Toxicology Program NIEHS, FDA, and NIOSH Members Technical Support Contractor Syracuse Research Corporation ITC Staff John D. Walker, Director Norma S. L. Williams, Executive Assistant TSCA Interagency Testing Committee (7401), Office of Pollution Prevention and Toxics, Environmental Protection Agency, 1200 Pennsylvania Ave., NW., Washington, DC 20460-0001; e-mail address: walker.johnd@epa.gov; url: http://www.epa.gov/ opptintr/itc/. Appendix A--Chemical Abstracts Service Registry Number (CAS No.), TSCA Inventory Names and Previous TSCA Section 8(d) Rule Sunset Dates of HPV Orphan Chemicals for Which the ITC is Requesting that the EPA Add to TSCA Section 8(a) and 8(d) Rules ---------------------------------------------------------------------------------------------------------------- Previous TSCA section 8(d) rule CAS No. TSCA Inventory Name sunset date ---------------------------------------------------------------------------------------------------------------- 62-56-6 Thiourea .................................. ------------------------------------------------------------------------------ 74-97-5 Methane, bromochloro- 6/1/1997 ------------------------------------------------------------------------------ 75-34-3 Ethane, 1,1-dichloro- 6/1/1997 ------------------------------------------------------------------------------ 75-46-7 Methane, trifluoro- .................................. ------------------------------------------------------------------------------ 77-76-9 Propane, 2,2-dimethoxy- .................................. ------------------------------------------------------------------------------ 81-07-2 1,2-Benzisothiazol-3(2H)-one, 1,1- .................................. dioxide ------------------------------------------------------------------------------ 81-16-3 1-Naphthalenesulfonic acid, 2-amino- .................................. ------------------------------------------------------------------------------ 81-84-5 1H,3H-Naphtho[1,8-cd]pyran-1,3-dione 6/30/1998 ------------------------------------------------------------------------------ 83-41-0 Benzene, 1,2-dimethyl-3-nitro- .................................. ------------------------------------------------------------------------------ 84-69-5 1,2-Benzenedicarboxylic acid, bis(2- 10/4/1992 methylpropyl) ester ------------------------------------------------------------------------------ 85-40-5 1H-Isoindole-1,3(2H)-dione, 3a,4,7,7a- .................................. tetrahydro- ------------------------------------------------------------------------------ 90-43-7 [1,1'-Biphenyl]-2-ol .................................. ------------------------------------------------------------------------------ 91-68-9 Phenol, 3-(diethylamino)- .................................. ------------------------------------------------------------------------------ 94-75-7 Acetic acid, (2,4-dichlorophenoxy)- .................................. ------------------------------------------------------------------------------ [[Page 7370]] 94-96-2 1,3-Hexanediol, 2-ethyl- .................................. ------------------------------------------------------------------------------ 95-94-3 Benzene, 1,2,4,5-tetrachloro- 10/4/1992 ------------------------------------------------------------------------------ 96-22-0 3-Pentanone .................................. ------------------------------------------------------------------------------ 96-23-1 2-Propanol, 1,3-dichloro- .................................. ------------------------------------------------------------------------------ 97-00-7 Benzene, 1-chloro-2,4-dinitro- .................................. ------------------------------------------------------------------------------ 98-09-9 Benzenesulfonyl chloride .................................. ------------------------------------------------------------------------------ 98-16-8 Benzenamine, 3-(trifluoromethyl)- .................................. ------------------------------------------------------------------------------ 98-56-6 Benzene, 1-chloro-4-(trifluoromethyl)- 4/29/1993 ------------------------------------------------------------------------------ 99-51-4 Benzene, 1,2-dimethyl-4-nitro- .................................. ------------------------------------------------------------------------------ 100-64-1 Cyclohexanone, oxime .................................. ------------------------------------------------------------------------------ 101-34-8 9-Octadecenoic acid, 12-(acetyloxy)-, .................................. 1,2,3-propanetriyl ester, (9Z,9'Z,9''Z,12R,12'R,12''R)- ------------------------------------------------------------------------------ 104-66-5 Benzene, 1,1'-[1,2- .................................. ethanediylbis(oxy)]bis- ------------------------------------------------------------------------------ 104-93-8 Benzene, 1-methoxy-4-methyl- .................................. ------------------------------------------------------------------------------ 107-39-1 1-Pentene, 2,4,4-trimethyl- .................................. ------------------------------------------------------------------------------ 107-40-4 2-Pentene, 2,4,4-trimethyl- .................................. ------------------------------------------------------------------------------ 107-45-9 2-Pentanamine, 2,4,4-trimethyl- .................................. ------------------------------------------------------------------------------ 110-18-9 1,2-Ethanediamine, N,N,N',N'-tetramethyl- .................................. ------------------------------------------------------------------------------ 110-33-8 Hexanedioic acid, dihexyl ester .................................. ------------------------------------------------------------------------------ 111-44-4 Ethane, 1,1'-oxybis[2-chloro- .................................. ------------------------------------------------------------------------------ 111-85-3 Octane, 1-chloro- .................................. ------------------------------------------------------------------------------ 111-91-1 Ethane, 1,1'-[methylenebis(oxy)]bis[2- .................................. chloro- ------------------------------------------------------------------------------ 118-90-1 Benzoic acid, 2-methyl- .................................. ------------------------------------------------------------------------------ 119-33-5 Phenol, 4-methyl-2-nitro- 6/30/1998 ------------------------------------------------------------------------------ 121-69-7 Benzenamine, N,N-dimethyl- 6/30/1998 ------------------------------------------------------------------------------ 121-82-4 1,3,5-Triazine, hexahydro-1,3,5-trinitro- .................................. ------------------------------------------------------------------------------ 124-63-0 Methanesulfonyl chloride .................................. ------------------------------------------------------------------------------ 127-68-4 Benzenesulfonic acid, 3-nitro-, sodium .................................. salt ------------------------------------------------------------------------------ 131-57-7 Methanone, (2-hydroxy-4- .................................. methoxyphenyl)phenyl- ------------------------------------------------------------------------------ 137-20-2 Ethanesulfonic acid, 2-[methyl[(9Z)-1- 12/28/1994 oxo-9- octadecenyl]amino]-, sodium salt ------------------------------------------------------------------------------ 138-25-0 1,3-Benzenedicarboxylic acid, 5-sulfo-, .................................. 1,3-dimethyl ester ------------------------------------------------------------------------------ 139-40-2 1,3,5-Triazine-2,4-diamine, 6-chloro- .................................. N,N'-bis(1-methylethyl)- ------------------------------------------------------------------------------ 140-08-9 Ethanol, 2-chloro-, phosphite (3:1) .................................. ------------------------------------------------------------------------------ 140-93-2 Carbonodithioic acid, O-(1-methylethyl) .................................. ester, sodium salt ------------------------------------------------------------------------------ 142-73-4 Glycine, N-(carboxymethyl)- .................................. ------------------------------------------------------------------------------ [[Page 7371]] 150-50-5 Phosphorotrithious acid, tributyl ester .................................. ------------------------------------------------------------------------------ 307-35-7 1-Octanesulfonyl fluoride, .................................. 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8- heptadecafluoro- ------------------------------------------------------------------------------ 330-54-1 Urea, N'-(3,4-dichlorophenyl)-N,N- .................................. dimethyl- ------------------------------------------------------------------------------ 460-00-4 Benzene, 1-bromo-4-fluoro- .................................. ------------------------------------------------------------------------------ 506-51-4 1-Tetracosanol .................................. ------------------------------------------------------------------------------ 506-52-5 1-Hexacosanol .................................. ------------------------------------------------------------------------------ 513-74-6 Carbamodithioic acid, monoammonium salt .................................. ------------------------------------------------------------------------------ 515-40-2 Benzene, (2-chloro-1,1-dimethylethyl)- .................................. ------------------------------------------------------------------------------ 529-33-9 1-Naphthalenol, 1,2,3,4-tetrahydro- .................................. ------------------------------------------------------------------------------ 529-34-0 1(2H)-Naphthalenone, 3,4-dihydro- .................................. ------------------------------------------------------------------------------ 542-75-6 1-Propene, 1,3-dichloro- .................................. ------------------------------------------------------------------------------ 542-92-7 1,3-Cyclopentadiene 6/30/1998 ------------------------------------------------------------------------------ 557-61-9 1-Octacosanol .................................. ------------------------------------------------------------------------------ 563-72-4 Ethanedioic acid, calcium salt (1:1) .................................. ------------------------------------------------------------------------------ 579-66-8 Benzenamine, 2,6-diethyl- .................................. ------------------------------------------------------------------------------ 590-19-2 1,2-Butadiene .................................. ------------------------------------------------------------------------------ 592-45-0 1,4-Hexadiene .................................. ------------------------------------------------------------------------------ 597-31-9 Propanal, 3-hydroxy-2,2-dimethyl- 6/30/1998 ------------------------------------------------------------------------------ 598-72-1 Propanoic acid, 2-bromo- .................................. ------------------------------------------------------------------------------ 617-94-7 Benzenemethanol, .alpha.,.alpha.- .................................. dimethyl- ------------------------------------------------------------------------------ 625-55-8 Formic acid, 1-methylethyl ester .................................. ------------------------------------------------------------------------------ 628-13-7 Pyridine, hydrochloride .................................. ------------------------------------------------------------------------------ 628-96-6 1,2-Ethanediol, dinitrate .................................. ------------------------------------------------------------------------------ 645-62-5 2-Hexenal, 2-ethyl- .................................. ------------------------------------------------------------------------------ 693-07-2 Ethane, 1-chloro-2-(ethylthio)- .................................. ------------------------------------------------------------------------------ 693-95-8 Thiazole, 4-methyl- .................................. ------------------------------------------------------------------------------ 756-80-9 Phosphorodithioic acid, O,O-dimethyl .................................. ester ------------------------------------------------------------------------------ 870-72-4 Methanesulfonic acid, hydroxy-, .................................. monosodium salt ------------------------------------------------------------------------------ 928-72-3 Glycine, N-(carboxymethyl)-, disodium .................................. salt ------------------------------------------------------------------------------ 939-97-9 Benzaldehyde, 4-(1,1-dimethylethyl)- 11/9/1993 ------------------------------------------------------------------------------ 1000-82-4 Urea, (hydroxymethyl)- 7/1/1993 ------------------------------------------------------------------------------ 1002-69-3 Decane, 1-chloro- .................................. ------------------------------------------------------------------------------ 1111-78-0 Carbamic acid, monoammonium salt .................................. ------------------------------------------------------------------------------ 1115-20-4 Propanoic acid, 3-hydroxy-2,2-dimethyl-, .................................. 3-hydroxy-2,2-dimethylpropyl ester ------------------------------------------------------------------------------ 1401-55-4 Tannins .................................. ------------------------------------------------------------------------------ [[Page 7372]] 1445-45-0 Ethane, 1,1,1-trimethoxy- .................................. ------------------------------------------------------------------------------ 1459-93-4 1,3-Benzenedicarboxylic acid, dimethyl .................................. ester ------------------------------------------------------------------------------ 1498-51-7 Phosphorodichloridic acid, ethyl ester 11/9/1993 ------------------------------------------------------------------------------ 1558-33-4 Silane, dichloro(chloromethyl)methyl- .................................. ------------------------------------------------------------------------------ 1646-75-9 Propanal, 2-methyl-2-(methylthio)-, .................................. oxime ------------------------------------------------------------------------------ 1691-99-2 1-Octanesulfonamide, N-ethyl- .................................. 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8- heptadecafluoro-N-(2-hydroxyethyl)- ------------------------------------------------------------------------------ 1738-25-6 Propanenitrile, 3-(dimethylamino)- .................................. ------------------------------------------------------------------------------ 1912-24-9 1,3,5-Triazine-2,4-diamine, 6-chloro-N- .................................. ethyl-N'-(1-methylethyl)- ------------------------------------------------------------------------------ 1918-02-1 2-Pyridinecarboxylic acid, 4-amino-3,5,6- .................................. trichloro- ------------------------------------------------------------------------------ 1929-82-4 Pyridine, 2-chloro-6-(trichloromethyl)- .................................. ------------------------------------------------------------------------------ 2152-64-9 Benzenamine, N-phenyl-4-[[4- .................................. (phenylamino)phenyl][4-(phenylimino)- 2,5-cyclohexadien-1-ylidene]methyl]-, monohydrochloride ------------------------------------------------------------------------------ 2210-79-9 Oxirane, [(2-methylphenoxy)methyl]- 10/4/1992 ------------------------------------------------------------------------------ 2372-45-4 1-Butanol, sodium salt .................................. ------------------------------------------------------------------------------ 2409-55-4 Phenol, 2-(1,1-dimethylethyl)-4-methyl- .................................. ------------------------------------------------------------------------------ 2425-54-9 Tetradecane, 1-chloro- .................................. ------------------------------------------------------------------------------ 2494-89-5 Ethanol, 2-[(4-aminophenyl)sulfonyl]-, .................................. hydrogen sulfate (ester) ------------------------------------------------------------------------------ 2524-03-0 Phosphorochloridothioic acid, O,O- .................................. dimethyl ester ------------------------------------------------------------------------------ 2611-00-9 3-Cyclohexene-1-carboxylic acid, 3- .................................. cyclohexen-1-ylmethyl ester ------------------------------------------------------------------------------ 2691-41-0 1,3,5,7-Tetrazocine, octahydro-1,3,5,7- .................................. tetranitro- ------------------------------------------------------------------------------ 2702-72-9 Acetic acid, (2,4-dichlorophenoxy)-, .................................. sodium salt ------------------------------------------------------------------------------ 2814-20-2 4(1H)-Pyrimidinone, 6-methyl-2-(1- .................................. methylethyl)- ------------------------------------------------------------------------------ 2905-62-6 Benzoyl chloride, 3,5-dichloro- .................................. ------------------------------------------------------------------------------ 2915-53-9 2-Butenedioic acid (2Z)-, dioctyl ester .................................. ------------------------------------------------------------------------------ 3039-83-6 Ethenesulfonic acid, sodium salt .................................. ------------------------------------------------------------------------------ 3088-31-1 Ethanol, 2-[2-(dodecyloxy)ethoxy]-, .................................. hydrogen sulfate, sodium salt ------------------------------------------------------------------------------ 3132-99-8 Benzaldehyde, 3-bromo- 6/30/1998 ------------------------------------------------------------------------------ 3338-24-7 Phosphorodithioic acid, O,O-diethyl .................................. ester, sodium salt ------------------------------------------------------------------------------ 3386-33-2 Octadecane, 1-chloro- .................................. ------------------------------------------------------------------------------ 3586-14-9 Benzene, 1-methyl-3-phenoxy- 6/30/1998 ------------------------------------------------------------------------------ 3710-84-7 Ethanamine, N-ethyl-N-hydroxy- .................................. ------------------------------------------------------------------------------ 3779-63-3 1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, .................................. 1,3,5-tris(6-isocyanatohexyl)- ------------------------------------------------------------------------------ 3965-55-7 1,3-Benzenedicarboxylic acid, 5-sulfo-, .................................. 1,3-dimethyl ester, sodium salt ------------------------------------------------------------------------------ 4035-89-6 Imidodicarbonic diamide, N,N',2-tris(6- 11/9/1993 isocyanatohexyl)- ------------------------------------------------------------------------------ 4080-31-3 3,5,7-Triaza-1- .................................. azoniatricyclo[3.3.1.13,7]decane, 1-(3- chloro-2-propenyl)-, chloride ------------------------------------------------------------------------------ [[Page 7373]] 4170-30-3 2-Butenal .................................. ------------------------------------------------------------------------------ 4300-97-4 Propanoyl chloride, 3-chloro-2,2- .................................. dimethyl- ------------------------------------------------------------------------------ 4316-73-8 Glycine, N-methyl-, monosodium salt .................................. ------------------------------------------------------------------------------ 4860-03-1 Hexadecane, 1-chloro- .................................. ------------------------------------------------------------------------------ 5026-74-4 Oxiranemethanamine, N-[4- .................................. (oxiranylmethoxy)phenyl]-N- (oxiranylmethyl)- ------------------------------------------------------------------------------ 5216-25-1 Benzene, 1-chloro-4-(trichloromethyl)- .................................. ------------------------------------------------------------------------------ 5460-09-3 2,7-Naphthalenedisulfonic acid, 4-amino- .................................. 5-hydroxy-, monosodium salt ------------------------------------------------------------------------------ 5915-41-3 1,3,5-Triazine-2,4-diamine, 6-chloro-N- .................................. (1,1-dimethylethyl)-N'-ethyl- ------------------------------------------------------------------------------ 6473-13-8 2-Naphthalenesulfonic acid, 6-[(2,4- .................................. diaminophenyl)azo]-3-[[4-[[4-[[7-[(2,4- diaminophenyl)azo]-1-hydroxy-3-sulfo-2- naphthalenyl]azo]phenyl]amino]-3- sulfophenyl]azo]-4-hydroxy-, trisodium salt ------------------------------------------------------------------------------ 6863-58-7 Butane, 2,2'-oxybis- .................................. ------------------------------------------------------------------------------ 6865-35-6 Octadecanoic acid, barium salt .................................. ------------------------------------------------------------------------------ 7320-37-8 Oxirane, tetradecyl- 10/40/1992 ------------------------------------------------------------------------------ 7446-81-3 2-Propenoic acid, sodium salt .................................. ------------------------------------------------------------------------------ 7795-95-1 1-Octanesulfonyl chloride .................................. ------------------------------------------------------------------------------ 8001-58-9 Creosote .................................. ------------------------------------------------------------------------------ 10265-69-7 Glycine, N-phenyl-, monosodium salt .................................. ------------------------------------------------------------------------------ 13749-94-5 Ethanimidothioic acid, N-hydroxy-, 6/30/1998 methyl ester ------------------------------------------------------------------------------ 13826-35-2 Benzenemethanol, 3-phenoxy- .................................. ------------------------------------------------------------------------------ 14143-60-3 2-Pyridinecarbonitrile, 4-amino-3,5,6- .................................. trichloro- ------------------------------------------------------------------------------ 14666-94-5 9-Octadecenoic acid (9Z)-, cobalt salt .................................. ------------------------------------------------------------------------------ 17103-31-0 Urea, sulfate (2:1) .................................. ------------------------------------------------------------------------------ 17321-47-0 Phosphoramidothioic acid, O,O-dimethyl .................................. ester ------------------------------------------------------------------------------ 17976-43-1 2,4,6,8,3,5,7- .................................. Benzotetraoxatriplumbacycloundecin- 3,5,7-triylidene, 1,9-dihydro-1,9-dioxo- ------------------------------------------------------------------------------ 19438-61-0 1,3-Isobenzofurandione, 5-methyl- .................................. ------------------------------------------------------------------------------ 19525-59-8 Glycine, N-phenyl-, monopotassium salt .................................. ------------------------------------------------------------------------------ 20068-02-4 2-Butenenitrile, 2-methyl-, (2Z)- .................................. ------------------------------------------------------------------------------ 20227-53-6 Phosphorous acid, 2-(1,1-dimethylethyl)- .................................. 4-[1-[3-(1,1-dimethylethyl)-4- hydroxyphenyl]-1-methylethyl]phenyl bis(4-nonylphenyl) ester ------------------------------------------------------------------------------ 20469-71-0 Hydrazinecarbodithioic acid, compd. with .................................. hydrazine (1:1) ------------------------------------------------------------------------------ 21351-39-3 Urea, sulfate (1:1) .................................. ------------------------------------------------------------------------------ 22527-63-5 Propanoic acid, 2-methyl-, 3- .................................. (benzoyloxy)-2,2,4-trimethylpentyl ester ------------------------------------------------------------------------------ 24448-09-7 1-Octanesulfonamide, .................................. 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8- heptadecafluoro-N-(2-hydroxyethyl)-N- methyl- ------------------------------------------------------------------------------ 24615-84-7 2-Propenoic acid, 2-carboxyethyl ester .................................. ------------------------------------------------------------------------------ [[Page 7374]] 24794-58-9 Formic acid, compd. with 2,2',2''- .................................. nitrilotris[ethanol] (1:1) ------------------------------------------------------------------------------ 25154-38-5 Piperazineethanol .................................. ------------------------------------------------------------------------------ 25168-05-2 Benzene, chloromethyl- .................................. ------------------------------------------------------------------------------ 25168-06-3 Phenol, (1-methylethyl)- 11/9/1993 ------------------------------------------------------------------------------ 25321-41-9 Benzenesulfonic acid, dimethyl- .................................. ------------------------------------------------------------------------------ 25383-99-7 Octadecanoic acid, 2-(1-carboxyethoxy)-1- .................................. methyl-2-oxoethyl ester, sodium salt ------------------------------------------------------------------------------ 25586-42-9 Phosphorous acid, tris(methylphenyl) .................................. ester ------------------------------------------------------------------------------ 25646-71-3 Methanesulfonamide, N-[2-[(4-amino-3- .................................. methylphenyl)ethylamino]ethyl]-, sulfate (2:3) ------------------------------------------------------------------------------ 26377-29-7 Phosphorodithioic acid, O,O-dimethyl .................................. ester, sodium salt ------------------------------------------------------------------------------ 26401-27-4 Phosphorous acid, isooctyl diphenyl .................................. ester ------------------------------------------------------------------------------ 26680-54-6 2,5-Furandione, dihydro-3-(octenyl)- .................................. ------------------------------------------------------------------------------ 27193-28-8 Phenol, (1,1,3,3-tetramethylbutyl)- 6/30/1998 ------------------------------------------------------------------------------ 28106-30-1 Benzene, ethenylethyl- .................................. ------------------------------------------------------------------------------ 28188-24-1 Octadecanoic acid, 2-(hydroxymethyl)-2- .................................. [[(1-oxooctadecyl)oxy]methyl]-1,3- propanediyl ester ------------------------------------------------------------------------------ 28777-98-2 2,5-Furandione, dihydro-3-(octadecenyl)- .................................. ------------------------------------------------------------------------------ 28908-00-1 Benzothiazole, 2-[(chloromethyl)thio]- .................................. ------------------------------------------------------------------------------ 30574-97-1 2-Butenenitrile, 2-methyl-, (2E)- .................................. ------------------------------------------------------------------------------ 32072-96-1 2,5-Furandione, 3-(hexadecenyl)dihydro- .................................. ------------------------------------------------------------------------------ 33509-43-2 1,2,4-Triazin-5(2H)-one, 4-amino-6-(1,1- .................................. dimethylethyl)-3,4-dihydro-3-thioxo- ------------------------------------------------------------------------------ 34689-46-8 Phenol, methyl-, sodium salt .................................. ------------------------------------------------------------------------------ 35203-06-6 Benzenamine, 2-ethyl-6-methyl-N- .................................. methylene- ------------------------------------------------------------------------------ 35203-08-8 Benzenamine, 2,6-diethyl-N-methylene- .................................. ------------------------------------------------------------------------------ 37439-34-2 2(1H)-Pyridinone, 3,5,6-trichloro-, .................................. sodium salt ------------------------------------------------------------------------------ 37734-45-5 Carbonochloridothioic acid, S- .................................. (phenylmethyl) ester ------------------------------------------------------------------------------ 37764-25-3 Acetamide, 2,2-dichloro-N,N-di-2- .................................. propenyl- ------------------------------------------------------------------------------ 38185-06-7 Benzenesulfonic acid, 4-chloro-3,5- .................................. dinitro-, potassium salt ------------------------------------------------------------------------------ 38321-18-5 Ethanol, 2-(2-butoxyethoxy)-, sodium .................................. salt ------------------------------------------------------------------------------ 39515-51-0 Benzaldehyde, 3-phenoxy- 6/30/1998 ------------------------------------------------------------------------------ 40630-63-5 1-Octanesulfonyl fluoride .................................. ------------------------------------------------------------------------------ 40876-98-0 Butanedioic acid, oxo-, diethyl ester, .................................. ion(1-), sodium ------------------------------------------------------------------------------ 51632-16-7 Benzene, 1-(bromomethyl)-3-phenoxy- 6/30/1998 ------------------------------------------------------------------------------ 52184-19-7 Phenol, 2,4-bis(1,1-dimethylpropyl)-6- .................................. [(2- nitrophenyl)azo]- ------------------------------------------------------------------------------ 52556-42-0 1-Propanesulfonic acid, 2-hydroxy-3-(2- .................................. propenyloxy)-, monosodium salt ------------------------------------------------------------------------------ 52663-57-7 Ethanol, 2-butoxy-, sodium salt .................................. ------------------------------------------------------------------------------ [[Page 7375]] 56038-89-2 Benzenamine, N-(1-ethylpropyl)-3,5- .................................. dimethyl- ------------------------------------------------------------------------------ 56803-37-3 Phosphoric acid, (1,1- 10/4/1992 dimethylethyl)phenyl diphenyl ester ------------------------------------------------------------------------------ 57693-14-8 Chromate(3-), bis[3-(hydroxy-.kappa.O)-4- .................................. [[2-(hydroxy-.kappa.O)-1- naphthalenyl]azo-.kappa.N1]-7-nitro-1- naphthalenesulfonato(3-)]-, trisodium ------------------------------------------------------------------------------ 61788-76-9 Alkanes, chloro .................................. ------------------------------------------------------------------------------ 61789-32-0 Fatty acids, coco, 2-sulfoethyl esters, .................................. sodium salts ------------------------------------------------------------------------------ 61789-85-3 Sulfonic acids, petroleum .................................. ------------------------------------------------------------------------------ 63302-49-8 Phosphorochloridous acid, bis(4- .................................. nonylphenyl) ester ------------------------------------------------------------------------------ 64742-24-1 Sludges (petroleum), acid .................................. ------------------------------------------------------------------------------ 64743-02-8 Alkenes, C>10 .alpha.- .................................. ------------------------------------------------------------------------------ 64743-03-9 Phenols (petroleum) .................................. ------------------------------------------------------------------------------ 64771-71-7 Paraffins (petroleum), normal C>10 .................................. ------------------------------------------------------------------------------ 65996-79-4 Solvent naphtha (coal) .................................. ------------------------------------------------------------------------------ 65996-80-7 Ammonia liquor (coal) .................................. ------------------------------------------------------------------------------ 65996-81-8 Fuel gases, coke-oven .................................. ------------------------------------------------------------------------------ 65996-82-9 Tar oils, coal .................................. ------------------------------------------------------------------------------ 65996-83-0 Extracts, coal tar oil alk. .................................. ------------------------------------------------------------------------------ 65996-86-3 Extract oils (coal), tar base .................................. ------------------------------------------------------------------------------ 65996-87-4 Extract residues (coal), tar oil alk. .................................. ------------------------------------------------------------------------------ 65996-89-6 Tar, coal, high-temp. .................................. ------------------------------------------------------------------------------ 65996-91-0 Distillates (coal tar), upper .................................. ------------------------------------------------------------------------------ 65996-92-1 Distillates (coal tar) .................................. ------------------------------------------------------------------------------ 66071-94-1 Corn, steep liquor .................................. ------------------------------------------------------------------------------ 68081-86-7 Phenol, nonyl derivs. .................................. ------------------------------------------------------------------------------ 68082-78-0 Lard, oil, Me esters .................................. ------------------------------------------------------------------------------ 68153-60-6 Fatty acids, tall-oil, reaction products .................................. with diethylenetriamine, acetates ------------------------------------------------------------------------------ 68187-41-7 Phosphorodithioic acid, O,O-di-C1-14- .................................. alkyl esters ------------------------------------------------------------------------------ 68187-57-5 Pitch, coal tar-petroleum .................................. ------------------------------------------------------------------------------ 68187-59-7 Coal, anthracite, calcined .................................. ------------------------------------------------------------------------------ 68188-18-1 Paraffin oils, chlorosulfonated, .................................. saponified ------------------------------------------------------------------------------ 68308-74-7 Amides, tall-oil fatty, N,N-di-Me .................................. ------------------------------------------------------------------------------ 68309-16-0 Fatty acids, tall-oil, 2-(2- .................................. hydroxyethoxy)ethyl esters ------------------------------------------------------------------------------ 68309-27-3 Fatty acids, tall-oil, sulfonated, .................................. sodium salts ------------------------------------------------------------------------------ 68334-01-0 Disulfides, alkylaryl dialkyl diaryl, .................................. petroleum refinery spent caustic oxidn. products ------------------------------------------------------------------------------ 68441-66-7 Decanoic acid, mixed esters with .................................. dipentaerythritol, octanoic acid and valeric acid ------------------------------------------------------------------------------ [[Page 7376]] 68442-60-4 Acetaldehyde, reaction products with .................................. formaldehyde, by-products from ------------------------------------------------------------------------------ 68442-77-3 2-Butenediamide, (2E)-, N,N'-bis[2-(4,5- .................................. dihydro-2-nortall-oil alkyl-1H-imidazol- 1-yl)ethyl] derivs. ------------------------------------------------------------------------------ 68476-80-2 Fats and Glyceridic oils, vegetable, .................................. deodorizer distillates ------------------------------------------------------------------------------ 68478-20-6 Residues (petroleum), steam-cracked .................................. petroleum distillates cyclopentadiene conc., C4-cyclopentadiene-free ------------------------------------------------------------------------------ 68512-63-0 Benzene, ethenyl-, distn. residues .................................. ------------------------------------------------------------------------------ 68513-62-2 Disulfides, C5-12-alkyl .................................. ------------------------------------------------------------------------------ 68514-41-0 Ketones, C12-branched .................................. ------------------------------------------------------------------------------ 68515-89-9 Barium, carbonate nonylphenol complexes .................................. ------------------------------------------------------------------------------ 68584-25-8 Benzenesulfonic acid, C10-16-alkyl .................................. derivs., compds. with triethanolamine ------------------------------------------------------------------------------ 68602-81-3 Distillates, hydrocarbon resin prodn. .................................. higher boiling ------------------------------------------------------------------------------ 68603-84-9 Carboxylic acids, C5-9 .................................. ------------------------------------------------------------------------------ 68608-59-3 Ethane, 1,2-dichloro-, manuf. of, by- .................................. products from, distn. lights ------------------------------------------------------------------------------ 68609-05-2 Cyclohexane, oxidized, non-acidic by- .................................. products, distn. lights ------------------------------------------------------------------------------ 68610-90-2 2-Butenedioic acid (2E)-, di-C8-18-alkyl .................................. esters ------------------------------------------------------------------------------ 68649-42-3 Phosphorodithioic acid, O,O-di-C1-14- .................................. alkyl esters ------------------------------------------------------------------------------ 68650-36-2 Aromatic hydrocarbons, C8, o-xylene-lean .................................. ------------------------------------------------------------------------------ 68782-97-8 Distillates (petroleum), hydrofined .................................. lubricating-oil ------------------------------------------------------------------------------ 68815-50-9 Octadecanoic acid, reaction products .................................. with 2-[(2-aminoethyl)amino]ethanol ------------------------------------------------------------------------------ 68909-77-3 Ethanol, 2,2'-oxybis-, reaction products .................................. with ammonia, morpholine derivs. residues ------------------------------------------------------------------------------ 68915-05-9 Fatty acids, tall-oil, low-boiling, .................................. reaction products with ammonia- ethanolamine reaction by-products ------------------------------------------------------------------------------ 68915-39-9 Cyclohexane, oxidized, aq. ext., sodium .................................. salt ------------------------------------------------------------------------------ 68918-16-1 Tar, coal, dried and oxidized .................................. ------------------------------------------------------------------------------ 68919-17-5 Hydrocarbons, C12-20, catalytic .................................. alkylation by-products ------------------------------------------------------------------------------ 68920-64-9 Disulfides, di-C1-2-alkyl .................................. ------------------------------------------------------------------------------ 68937-29-1 1,6-Hexanediol, distn. residues .................................. ------------------------------------------------------------------------------ 68937-69-9 Carboxylic acids, C6-18 and C5-15-di- .................................. ------------------------------------------------------------------------------ 68937-70-2 Carboxylic acids, C6-18 and C8-15-di- .................................. ------------------------------------------------------------------------------ 68937-72-4 Carboxylic acids, di-, C4-11 .................................. ------------------------------------------------------------------------------ 68953-70-8 Oxirane, reaction products with ammonia, .................................. distn. residues ------------------------------------------------------------------------------ 68953-80-0 Benzene, mixed with toluene, .................................. dealkylation product ------------------------------------------------------------------------------ 68955-37-3 Acid chlorides, tallow, hydrogenated .................................. ------------------------------------------------------------------------------ 68955-76-0 Aromatic hydrocarbons, C9-16, biphenyl .................................. deriv.-rich ------------------------------------------------------------------------------ 68955-96-4 Disulfides, dialkyl and di-Ph, naphtha .................................. sweetening ------------------------------------------------------------------------------ [[Page 7377]] 68987-41-7 Benzene, ethylenated .................................. ------------------------------------------------------------------------------ 68987-66-6 Ethene, hydrated, by-products from .................................. ------------------------------------------------------------------------------ 68988-22-7 1,4-Benzenedicarboxylic acid, dimethyl .................................. ester, manuf. of, by-products from ------------------------------------------------------------------------------ 68988-99-8 Phenols, sodium salts, mixed with sulfur .................................. compounds, gasoline alk. scrubber residues ------------------------------------------------------------------------------ 68990-61-4 Tar, coal, high-temp., high-solids .................................. ------------------------------------------------------------------------------ 68990-65-8 Fats and Glyceridic oils, vegetable, .................................. reclaimed ------------------------------------------------------------------------------ 70024-67-8 Benzenesulfonic acid, C16-24-alkyl .................................. derives. ------------------------------------------------------------------------------ 70084-98-9 Terpenes and Terpenoids, C10-30, distn. .................................. residues ------------------------------------------------------------------------------ 70693-50-4 Phenol, 2,4-bis(1-methyl-1-phenylethyl)- .................................. 6-[(2- nitrophenyl)azo]- ------------------------------------------------------------------------------ 70851-08-0 Amides, coco, N-[3- .................................. (dimethylamino)propyl], alkylation products with sodium 3-chloro-2- hydroxypropanesulfonate ------------------------------------------------------------------------------ 71077-05-9 Ethanol, 2,2'-oxybis-, reaction products .................................. with ammonia, morpholine product tower residues ------------------------------------------------------------------------------ 72162-28-8 2-Propanone, reaction products with .................................. phenol ------------------------------------------------------------------------------ 72854-27-4 Tannins, reaction products with sodium .................................. bisulfite, sodium polysulfide and sodium sulfite ------------------------------------------------------------------------------ 73665-18-6 Extract residues (coal), tar oil alk., .................................. naphthalene distn. residues ------------------------------------------------------------------------------ 83864-02-2 Nickel, bis[(cyano-C)triphenylborato(1-)- .................................. N]bis(hexanedinitrile-N,N')- ------------------------------------------------------------------------------ 84501-86-0 Hexanedioic acid, esters with high- .................................. boiling C6-10-alkene hydroformylation products ------------------------------------------------------------------------------ 90640-80-5 Anthracene oil .................................. ------------------------------------------------------------------------------ 90640-86-1 Distillates (coal tar), heavy oils .................................. ------------------------------------------------------------------------------ 119345-02-7 Benzene, 1,1'-oxybis-, tetrapropylene .................................. derivs. ------------------------------------------------------------------------------ 125997-20-8 Phosphoric acid, mixed 3-bromo-2,2- .................................. dimethylpropyl and 2-bromoethyl and 2- chloroethyl esters ---------------------------------------------------------------------------------------------------------------- [FR Doc. 05-2714 Filed 2-10-05; 8:45 am] BILLING CODE 6560-50-S